High-performance liquid chromatographic determination of chitin in the snow crab, Chionoecetes opilio

A HPLC method was developed for the determination of glucosamine in crab shells. The amount of glucosamine residue can be used to estimate the amount of chitin in analyzed material. Crab samples were hydrolysed with 6M HCl at 100 degrees C for 13 h and the released glucosamine was determined by HPLC using refractive index (RI) detection. Separations were performed using an ODS-2 column with an isocratic mobile phase consisting of 10% methanol, 90% hexanesulfonate, pH 2.1. Glucosamine identification was carried out not only on basis of retention time, but also with respect to mass spectra, which were acquired by HPLC-MS.     

Proposals for Fabrication of Long-Period Grating in LiNbO3 Strip Waveguides

The structure of a strip LiNbO3 waveguide clad with a planar LiNbOa waveguide is proposed to fabricate a long-period waveguide grating （LPWG）. It is shown theoretically that an LPWG device based on such a special LiNbOa waveguide structure is of the merit of thermal stability. The methods for fabrication of planar waveguide, channel waveguide and grating are suggested and discussed. Detailed design consideration is exemplified based on a soft-proton-exchange planar waveguide clad Ti-diffused LiNbOa （Z-cut） strip waveguide.     

Long period grating in/on planar and channel waveguides: A theory description

A comprehensive, complete theory suitable for a long period grating (LPG) on/in a planar or channel waveguide is described on the basis of coupled mode theory. The theory aims at key characteristic parameters with respect to the effect of the LPG, including resonance wavelength, transmission power of the guided mode in the waveguide, full-width at half-maximum (FWHM) of the power attenuation band in transmission spectrum of the guided mode, and coupling coefficient between a guided and a coupled mode. The type of the grating including relief and index modulation, different polarization state combinations of the guided mode and the resonant mode, and slanted grating structure are considered in this theory. The influences of the coupling between two guided modes and between a guided mode and a substrate mode are discussed. The role of cladding layer in a long period waveguide grating is demonstrated in particular. Finally, the expressions for the sensitivity of resonance wavelength as a function of external temperature, pressure and surrounding refractive index are derived.     

Research on the influence of fabrication parameters on the performance of buried ion-exchanged glass waveguides using the variational method

The variational method is proposed to analyze the influence of the fabrication parameters on the performance of buried K⁺–Na⁺ ion-exchanged Er³⁺–Yb³⁺ ions co-doped glass waveguide. The unknown parameters of the Hermite–Gaussian functions as the trial field distribution are determined based on the scalar variational principle. It is demonstrated that the results calculated in this paper agree with those measured in the experiment. The mode dimensions, the effective refractive index, and the overlap factor as the functions of the fabrication parameters are investigated. These results of the variational analysis are useful for the design and optimization of Er³⁺–Yb³⁺ ions co-doped waveguides.     

Estimation of Mean and Covariance Operator for Banach Space Valued Autoregressive Processes with Dependent Innovations

In this paper we study autoregressive processes of order 1 with values in a separable Banach space it B. Such ARB(1)-processes are defined by the recursion equation

Regeneration amplitude of KS0 from KL0 in carbon

We have measured the transmission regeneration amplitude for carbon. The invariant amplitude $\text{[?(0) ?}\text{?}\text{(0)]/P}$ varies from 5.909 ± 0.066 mb at 4.5 GeV/c to 3.933 ± 0.152 mb at 9.5 GeV/c. The results agree with optical model calculations using measured kaon-nucleon total cross sections. The data also provide a value for the ω trajectory intercept α_ω(0) = 0.42 ± 0.04.     

Secondary-ion-mass spectrometry study on near-stoichiometric LiNbO3 strip waveguide fabricated by vapour transport equilibration and Ti co-diffusion

Secondary-ion-mass spectrometry was applied to study Ti-concentration profiles in the depth direction and on the surface of near-stoichiometric (NS) Ti:LiNbO₃ strip waveguides fabricated using vapour transport equilibration (VTE) and co-diffusion of Ti-metal strips. Results show that the profile of Ti concentration along the width direction on the waveguide surface can be well fitted by a sum of two error functions, while, in the depth direction, the Ti concentration follows either a complementary error function or a generalized Gaussian function. Surface Ti concentration, 1/e width and depth, mean diffusivities along the width and depth directions of the guide are, respectively, 1.04?×?10²¹?cm^–3, 8.5?µm, 6.3?µm, 0.18 and 0.1?µm²/h. Two-dimensional refractive index profile in the NS waveguides is indirectly constructed by assuming linearity between Ti-induced index change and Ti concentration. The surface refractive index increments at 1545?nm, Δn_o and Δn_e , are evaluated to be 3.132?×?10^–3 and 1.186?×?10^–2, respectively. All of the above-mentioned diffusion and optical parameters are compared with the corresponding data of the common congruent Ti:LiNbO₃ waveguide or NS waveguide fabricated starting from a NS substrate. The rationality of the assumed linear relationship between the index change and the Ti concentration is discussed. The results show that the assumed linearity remains controversial, and all expressions and data with regard to the refractive index are the approximate results and need to be verified by direct measurement on refractive index.     

A geometric proof of a theorem on antiregularity of generalized quadrangles

A geometric proof is given in terms of Laguerre geometry of the theorem of Bagchi, Brouwer and Wilbrink, which states that if a generalized quadrangle of order s > 1 has an antiregular point then all of its points are antiregular.     

Radiation stability of nanoscale ferromagnetic memory elements

Computer-simulation data on the radiation-induced processes in nanoscale ferromagnetic clusters exposed to charged and neutral particles are presented. An instability-zone radius that characterizes the material’s radiation stability is estimated for an atom knocked out from a lattice site. Temperature and thermoelastic effects in the clusters and their influence on the defect structure of the irradiated objects are considered.     

Gain properties of the transition emissions near the second telecommunication window in Ho3+-doped multicomponent heavy-metal gallate glasses

Efficient infrared emissions near the second telecommunication window in Ho³⁺-doped multicomponent heavy-metal gallate (MHG) glasses have been observed. The maximum stimulated emission cross-sections are calculated to be 2.94×10^?21 and 2.08×10^?21 cm² for 1200 and 1390 nm emissions, respectively. Excitation spectra reveal that the 642 and 538 nm wavelengths are practical pumping conditions for 1.2 and 1.39 μm emissions, respectively. Gain cross-sections are evaluated and positive gain bands have been anticipated. The theoretical gain results indicate that the appealing infrared emissions near the second telecommunication window from Ho³⁺-doped MHG glasses with low maximum phonon energy of ～660 cm^?1 make them attractive in developing ～1.2 μm and E-band (1360–1460 nm) optical amplifiers.